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HRID1695646

反应详情

EQUATION

反应方程式

HRID 1695646 的结构方程式

REACTANTS

反应物

2
结构：NCCOc1ccccc1
HCID15651

2-Phenoxyethanamine

C8H11NO

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc2c(c1)COC(NCCOc1ccccc1)=N2
HCID178526445

未命名化合物

收率 96%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (1.95 g, 6.0 mmol; HPLC: 4.446 min) and 2-phenoxyethylamine (CAS 1758-46-9) (807 mg, 6.0 mmol; HPLC: 0.381 min) according to the procedure described for Example 1. Obtained the title compound as a yellow solid (1.80 g, 96%, HPLC 1.789 min), MS (ISP) m/e=314.0 [(M+H)+].