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HRID1695648

反应详情

EQUATION

反应方程式

HRID 1695648 的结构方程式

REACTANTS

反应物

2
结构：NC1CCCCCC1
HCID2899

Cycloheptanamine

C7H15N

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc2c(c1)COC(NC1CCCCCC1)=N2
HCID178526442

未命名化合物

收率 100%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (5.0 g, 15 mmol) and cycloheptylamine (1.8 g, 16 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow foam (4.3 g, 100%), MS (ISP) m/e=288.3 [(M−H)+].