HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptylamine → HCID 178526442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptylamine | HCID 2899 | — |
| Reactant | tert-Butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane | HCID 46855450 | — |
| Product | HCID 178526442 | HCID 178526442 | 100% |
Reaction Steps
Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (5.0 g, 15 mmol) and cycloheptylamine (1.8 g, 16 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow foam (4.3 g, 100%), MS (ISP) m/e=288.3 [(M−H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-d996c924fbaf432c8e0ef7f060404359 |
| Source note | uspto-grants-2012_04 |