HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178420323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 178507250 | HCID 178507250 | — |
| Product | HCID 178420323 | HCID 178420323 | 96.2% |
Reaction Steps
Prepared from N2-cycloheptyl-4H-benzo[d][1,3]oxazine-2,6-diamine (example 92) (200 mg, 0.77 mmol) and benzaldehyde (90 mg, 0.85 mmol) according to the procedure described for example 88. Obtained the title compound as a yellow oil (259 mg, 96%), MS (ISP) m/e=350.5 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-90085e01e0cb48978b88ace10552e501 |
| Source note | uspto-grants-2012_04 |