HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 178527454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | HCID 178507250 | HCID 178507250 | — |
| Product | HCID 178527454 | HCID 178527454 | 5.5% |
Reaction Steps
Prepared from N2-cycloheptyl-4H-benzo[d][1,3]oxazine-2,6-diamine (example 92) (200 mg, 0.77 mmol) and benzenesulfonyl chloride (136 mg, 0.77 mmol) according to the procedure described for example 27. Obtained the title compound as a white foam (17 mg, 5.5%), MS (ISP) m/e=400.3 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5294fe27bbc24faeaacb63e25d3faf3a |
| Source note | uspto-grants-2012_04 |