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HRID1695669

反应详情

EQUATION

反应方程式

HRID 1695669 的结构方程式

REACTANTS

反应物

2
结构：Nc1cccc(C2CC2)c1
HCID12032139

3-Cyclopropylaniline

C9H11N

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc2c(c1)COC(Nc1cccc(C3CC3)c1)=N2
HCID67277073

未命名化合物

收率 74%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (5.8 g, 18 mmol) and 3-cyclopropyl-phenylamine (2.5 g, 19 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow foam (4.1 g, 74%), MS (ISP) m/e=310.5 [(M+H)+].