huagongshe.com
HRID1695697

反应详情

EQUATION

反应方程式

HRID 1695697 的结构方程式

REACTANTS

反应物

2
结构：NC1CCCCCCC1
HCID2903

Cyclooctanamine

C8H17N

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc2c(c1)COC(NC1CCCCCCC1)=N2
HCID178526443

未命名化合物

收率 87.9%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (4.0 g, 12 mmol) and cyclooctylamine (1.6 g, 12 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow viscous oil (3.2 g, 83%), MS (ISP) m/e=304.1 [(M+H)+].