HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58255828, compound → HCID 58255733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58255828 | HCID 58255828 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 58255733 | HCID 58255733 | — |
Reaction Steps
6-(3-Methylphenyl)-4-nitro-2-(tetrahydro-2H-pyran-2-yl)-2H-indazole (422 mg, 1.25 mmol) was dissolved in ethyl acetate (25 ml) and reduced using the H-cube (available from ThalesNano) with a Pd/C catalyst cartridge at a pressure of up to 80 bar. The solvent was removed in vacuo to give the title compound, 286 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163743B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-4c0ffdce15534056bad9fd015d56ee03 |
| Source note | uspto-grants-2012_04 |