HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67273710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 67274196 | HCID 67274196 | — |
| Product | HCID 67273710 | HCID 67273710 | — |
Reaction Steps
A mixture of 0.099 g 6-amino-4-methylsulfanyl-pyridine-2-carboxylic acid methyl ester in 4 ml 25% aqueous ammonia was stirred at room temperature for 24 h. The solid was collected by filtration washed with water and dried to constant weight to yield 0.070 g of the title compound as white crystals melting at 158-159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163778B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-1290526803ca448985a184b120916241 |
| Source note | uspto-grants-2012_04 |