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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1696781Generated: November 2, 2026

Methylamine → HCID 67274430, compound

https://huagongshe.com/reaction/1696781

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 67274196HCID 67274196—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67274430HCID 67274430—

Reaction Steps

A solution of 0.099 g 6-amino-4-methylsulfanyl-pyridine-2-carboxylic acid methyl ester in 2 ml methylamine 2M in tetrahydrofuran was kept at room temperature for 24 h. The solvents were evaporated and the residue was recrystallized from water to yield 0.054 g of the title compound as white crystals melting at 89-91° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08163778B2
Source datasetuspto-grants-2012_04
ORD IDord-cc98ba1b58a342768e820832139fa356
Source noteuspto-grants-2012_04