HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 67274430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 67274196 | HCID 67274196 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67274430 | HCID 67274430 | — |
Reaction Steps
A solution of 0.099 g 6-amino-4-methylsulfanyl-pyridine-2-carboxylic acid methyl ester in 2 ml methylamine 2M in tetrahydrofuran was kept at room temperature for 24 h. The solvents were evaporated and the residue was recrystallized from water to yield 0.054 g of the title compound as white crystals melting at 89-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163778B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-cc98ba1b58a342768e820832139fa356 |
| Source note | uspto-grants-2012_04 |