HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67275357, compound → HCID 67275055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67275357 | HCID 67275357 | — |
| Solvent | Lithium Hydroxide | HCID 3939 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67275055 | HCID 67275055 | — |
Reaction Steps
A solution of Example 1E (332 mg) in 1M LiOH (3 mL) and THF (7 mL) was stirred at ambient temperature for 18 hours, diluted with dichloromethane, washed with 1M HCl, and dried (Na2SO4), filtered, and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ce61f28ed72b42a4bfdb5ed8002fb96e |
| Source note | uspto-grants-2012_04 |