HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminoazetidine, 3-BOC protected → HCID 67274679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminoazetidine, 3-BOC protected | HCID 1519405 | — |
| Reactant | HCID 87333591 | HCID 87333591 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67274679 | HCID 67274679 | — |
Reaction Steps
A solution of Example 7C (0.3 g) and 3-(tert-butoxycarbonylamino)azetidine (0.46 g) in dichloromethane (60 mL) was stirred for 2 hours, diluted with dichloromethane, washed with water, 10% citric acid, and brine, and dried (MgSO4), filtered, and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-97f89316e5d545e59d6d4f1544990117 |
| Source note | uspto-grants-2012_04 |