HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 11844216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 11328534 | HCID 11328534 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11844216 | HCID 11844216 | — |
Reaction Steps
A solution of Example 51B (17.9 g) in THF (750 mL) and methanol (70 mL) was treated with 1M LiOH (196 mL), stirred for 1.5 hours, and filtered. The filtrant was dissolved in 2:1 methanol/water (1.5 L), and this solution was treated with 1M HCl and water (500 mL total) and filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-180fa440c2f24d9ca2ac96eb1a17445d |
| Source note | uspto-grants-2012_04 |