HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 67275167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 67275302 | HCID 67275302 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67275167 | HCID 67275167 | — |
Reaction Steps
A suspension of EXAMPLE 66A (0.71 g) in THF (100 mL) and methanol (50 mL) at reflux was treated with 1M LiOH (100 mL), stirred for 3 hours, concentrated to half volume, acidified with 10% citric acid, and filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-7bd0c3e232d84a38b3d1399af456a01a |
| Source note | uspto-grants-2012_04 |