HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 67275514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 86615483 | HCID 86615483 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67275514 | HCID 67275514 | — |
Reaction Steps
A solution of Example 73C (210 mg), potassium carbonate (150 mg), and pyrrolidine (113 μl) in dichloromethane was stirred for 3 days, treated with potassium carbonate (150 mg) and pyrrolidine (113 μL), stirred for 3 more days, and concentrated; and the concentrate was purified by flash column chromatography on silica gel with a methanol/dichloromethane gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-bf16d9845b0849bb83fadaa65153f053 |
| Source note | uspto-grants-2012_04 |