HCID 67275514, compound → HCID 10244293, compound

Participants

Reaction Steps

A solution of Example 74A (63.2 mg) in ethanol (2.5 mL) and 6M HCl (2.5 mL) was heated in a sealed tube at 130° C. for 18 hours then cooled, diluted with diethyl ether, and filtered. NMR (300 MHz, DMSO-d6) δ 8.43 (s, 1H), 8.22 (m, 1H), 6.80 (m, 1H), 3.55 (m, 4H), 2.00 (m, 4H).

Provenance & Evidence