HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 10427221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 67275274 | HCID 67275274 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10427221 | HCID 10427221 | — |
Reaction Steps
A solution of Example 79A (128 mg) in 1:1 6M HCl/ethanol (15 mL) was refluxed for 24 hours then cooled, diluted with water, and filtered. NMR (300 MHz, DMSO) δ 15.22 (s, 1H), 13.11 (br s, 1H), 8.47 (s, 1H), 8.38 (s, 1H), 3.84-3.80 (m, 4H), 1.95-1.91 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163769B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-4a195a0e1ae14109a8eb82a0052eca03 |
| Source note | uspto-grants-2012_04 |