HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanol, 1-amino-2-methyl- → HCID 59846167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanol, 1-amino-2-methyl- | HCID 95102 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 4-Formylbenzene-1-sulfonyl chloride | HCID 2759210 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59846167 | HCID 59846167 | — |
Reaction Steps
To a solution of 4-formyl-benzene sulfonyl chloride (1.0 g) in MeOH was added NaHCO3 (0.425 g), followed by 1-amino-2-methylpropan-2-ol (0.566 g). The reaction mixture was stirred for 1 h at RT, then filtered through Celite and the solvent removed under reduced pressure to provide 4-formyl-N-(2-hydroxy-2-methylpropyl)-benzene sulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163906B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-84e19fda845941afaeadf147790c95b7 |
| Source note | uspto-grants-2012_04 |