Lithium hydroxide, monohydrate → HCID 57572049, compound

HRID 1697226Notes

Reaction equation

HRID 1697226 reaction equation
[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O:6]C)=[O:5].O.[OH-].[Li+:12]>CO.O>[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O-:6])=[O:5].[Li+:12]

Participants

5

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 19792887Methyl 2-methoxybutanoate

Product 1

HCID 57572049HCID 57572049, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

In a 15-mL RBF was dissolved methyl 2-methoxybutanoate (0.027 g, 0.20 mmol) in methanol (0.75 mL). A solution of lithium hydroxide monohydrate (0.0086 g, 0.20 mmol) in water (0.75 mL) was added, and the mixture was stirred overnight. The mixture was concentrated to afford the title compound.

Workup

  1. concentrationThe mixture was concentrated

Sources & evidence

ORD record
ord-87b39e8f3bf54b18b93c2f4f969fdc53
Source dataset
uspto-grants-2012_04
Patent number
US08163909B2

Reaction notes

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