HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenyl chloroformate → HCID 46946608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenyl chloroformate | HCID 2733256 | — |
| Reactant | HCID 66770259 | HCID 66770259 | — |
| Product | HCID 46946608 | HCID 46946608 | — |
Reaction Steps
(2S,4R)-4-(2-chloro-benzenesulfonyl)-pyrrolidine-2-carboxylic acid (1-cyano-cyclopropyl)-amide hydrochloride from experiment K4 was acylated with 4-fluorophenyl chloroformate in analogy to experiment L21 to give (2S,4R)-4-(2-chloro-benzenesulfonyl)-2-(1-cyano-cyclopropylcarbamoyl)-pyrrolidine-1-carboxylic acid 4-fluoro-phenyl ester as a colorless oil. MS: 492.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163793B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-19fd87a6f3ce415d8af08656a1b9f54a |
| Source note | uspto-grants-2012_04 |