HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylhydrazine monohydrochloride → HCID 66770715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylhydrazine monohydrochloride | HCID 81889 | — |
| Reactant | (2S,4R)-1-(3-oxo-thiobutyryl)-4-(2-trifluoromethyl-benzenesulfonyl)-pyrrolidine-2-carboxylic acid methyl ester | HCID 86646823 | — |
| Product | HCID 66770715 | HCID 66770715 | — |
Reaction Steps
In analogy to the procedure described in example 192 h, (2S,4R)-1-(3-oxo-thiobutyryl)-4-(2-trifluoromethyl-benzenesulfonyl)-pyrrolidine-2-carboxylic acid methyl ester (example 192 g) was reacted with tert-butylhydrazine hydrochloride (CAS Reg. No. 7400-27-3) to give the title compound as brown solid. MS (ESI): m/z=474.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163793B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-a7be6ae2539d4c15bab1f9ea15ea2a64 |
| Source note | uspto-grants-2012_04 |