HRID1697752

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID136200

4-(Trifluoromethyl)phenylhydrazine

C7H7F3N2

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1C(=S)CC(C)=O

HCID86646864

未命名化合物

PRODUCTS

生成物

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)CC2CC2)CN1c1cc(C)nn1-c1ccc(C(F)(F)F)cc1

HCID67278369

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 192 h, (2S,4R)-4-cyclopropylmethanesulfonyl-1-(3-oxo-thiobutyryl)-pyrrolidine-2-carboxylic acid methyl ester (example 445c) was reacted with 4-(trifluoromethyl)phenylhydrazine (CAS Reg. No. 368-90-1) to give the title compound as brown solid. MS (ESI): m/z=472.6 [M+H]+.