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HRID1697776

反应详情

EQUATION

反应方程式

HRID 1697776 的结构方程式

REACTANTS

反应物

2
结构：NNCCc1ccccc1.O=S(=O)(O)O
HCID61100

Phenylethylhydrazine sulfate

C8H14N2O4S

结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)c2ccc(F)cc2Cl)CN1C(=S)CC(C)=O
HCID86646870

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@@H]1C[C@@H](S(=O)(=O)c2ccc(F)cc2Cl)CN1c1cc(C)nn1CCc1ccccc1
HCID66772109

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 192 h, (2S,4R)-methyl 4-(2-chloro-4-fluorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate (example 464 a) was reacted with 2-phenethyl-hydrazine sulfate (CAS Reg. No. 56-51-4) to give the title compound as yellow oil. MS (ESI): m/z=506.1 [M+H]+.