Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 57012192 | HCID 57012192 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131729659 | HCID 131729659 | — |
Reaction Steps
In a light-protected flask and under N2 atmosphere, 4.4 g of 60% sodium hydride and 88 ml of dimethylformamide were mixed. To this mixture, a solution containing 8.1 g of mercaptomethylcyclopropylacetic acid and 20 ml of dimethylformamide was added while maintaining the temperature at 0-5° C. The reaction mixture was kept at this temperature for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08163924B2 |
|---|
| Source dataset | uspto-grants-2012_04 |
|---|
| ORD ID | ord-3c51c4e5afc948f790faf9075c64b29a |
|---|
| Source note | uspto-grants-2012_04 |
|---|
