HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-1-methylpyridin-2(1H)-one → HCID 59239068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-1-methylpyridin-2(1H)-one | HCID 13024027 | — |
| Reactant | 1-Ethyl-3-(4-(4-morpholino-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-2-yl) phenyl)urea | HCID 46913071 | — |
| Product | HCID 59239068 | HCID 59239068 | — |
Reaction Steps
The compound was prepared following the general procedure in Example 289, substituting 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline for 1-ethyl-3-(4-(4-morpholino-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-2-yl)phenyl)urea and substituting 2-Bromo-6-benzyloxypyridine for 5-bromo-1-methylpyridin-2(1H)-one: LC-MS m/z=490 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163763B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-d24d854592cd4fe7b384ad556905692c |
| Source note | uspto-grants-2012_04 |