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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1698217Generated: October 31, 2026

Hydrochloric Acid → HCID 66727315, compound

https://huagongshe.com/reaction/1698217

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant1,4-DioxaneHCID 31275—
ReactantHCID 66727467HCID 66727467—
SolventMethanolHCID 887—
ProductHCID 66727315HCID 66727315—

Reaction Steps

To a solution of 2-methyl-propane-2-sulfinic acid [(S)-1-(3-bromo-isoxazol-5-yl)-propyl]amide (17.5 mg, 0.0566 mmol) in MeOH (1 mL) was added a 4 M solution of HCl in dioxane (0.70 mL, 0.28 mmol) dropwise. After 2.5 hours, the mixture was concentrated in vacuo to afford the title compound which was used with out purification. MS m/z 188.24 (M−53), 190.20 (M+2−53).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08163918B2
Source datasetuspto-grants-2012_04
ORD IDord-7deac49ed5c247e4be942cd0d0edd503
Source noteuspto-grants-2012_04