HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → N-Methylbenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Benzene, (3-chloro-1-propenyl)- | HCID 94242 | — |
| Product | N-Methylbenzylamine | HCID 7669 | — |
Reaction Steps
The N-methylaminomethyl polystyrene resin is prepared as follows: To liquid methylamine, kept below −20° C., chloromethylstyrene copolymer (Merrifield resin) is added (˜1 g of resin per 10 ml of methylamine). The suspension is shaken in a pressure bottle at RT for 14 h. The resin is filtered off and washed with DMA (2×), H2O (2×), DMA (1×), CH3OH (2×), CH2Cl2 (3×), CH3OH (2×) and dried under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163773B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-554ae9f5b41d4bd29cf005d7a9cb373f |
| Source note | uspto-grants-2012_04 |