HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-methylpropane → HCID 67276389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 66671971 | HCID 66671971 | — |
| Product | HCID 67276389 | HCID 67276389 | 30% |
Reaction Steps
In a manner analogous to example 1 c, the process is carried out by a reaction of 4 g (16 mmol) of (4-bromo-2-tert-butylphenyl)ethylamine (example 1b) with 1.4 g (34 mmol) of 60% sodium hydride and with 3.7 ml (34 mmol) of 1-bromo-2-methylpropane. 1.5 g of (4-bromo-2-tert-butylphenyl)ethylisobutylamine are obtained in the form of an oil (yield=30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163952B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-7747337ac40544be8b6dba637e52f9e9 |
| Source note | uspto-grants-2012_04 |