HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 18322430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 14561225 | HCID 14561225 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18322430 | HCID 18322430 | 90% |
Reaction Steps
Ex-8e) Following the procedure described in Tetrahedron Lett Vol.21, 4263, (1980) partial saponification of 10.2 g of ethyl-2-acetylamino-6-t-butyloxycarbonylamino-2-ethoxycarbonyl-4-hexynoate is carried out in ethanol with 1.5 equivalent of KOH in water at 20-25° C. for 3 h to give 2-Acetylamino-6-t-butyloxycarbonylamino-2-ethoxycarbonyl-4-hexynoic acid in 90% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344483B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-a7453241ad094f17bf8010beca4d65ee |
| Source note | uspto-grants-2002_02 |