Hydrochloric Acid → HCID 14235670, compound

HRID 1698881Notes

Reaction equation

HRID 1698881 reaction equation
[C:1]([NH:4][CH:5]([CH2:9][C:10]#[C:11][CH2:12][NH:13]C(OC(C)(C)C)=O)[C:6]([OH:8])=[O:7])(=[O:3])[CH3:2].Cl>C(O)(=O)C.O1CCOCC1>[C:1]([NH:4][CH:5]([CH2:9][C:10]#[C:11][CH2:12][NH2:13])[C:6]([OH:8])=[O:7])(=[O:3])[CH3:2]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 15080570HCID 15080570, compound

Product 1

HCID 14235670HCID 14235670, compound

Reagents, catalysts & solvents 2

HCID 176Acetic AcidSolventHCID 312751,4-DioxaneSolvent

Procedure

Ex-8g) 10 g of 2-Acetylamino-6-t-butyloxycarbonylamino-4-hexynoic acid is taken up in 50 mL of acetic acid and 25 mL of 4N HCl in dioxane and stirred for 2 h at 25° C. The reaction mixture is stripped to dryness to give 2-Acetylamino-6-amino-4-hexynoic acid.

Sources & evidence

ORD record
ord-9beac6a085074d32a69db5df223ecd72
Source dataset
uspto-grants-2002_02
Patent number
US06344483B1

Reaction notes

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