HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 22246767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-(3,5-Dichlorophenoxy)ethylamine | HCID 49991 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22246767 | HCID 22246767 | — |
Reaction Steps
The title compound was prepared from 2-(3,5-dichloro-phenoxy)-ethylamine, Et3N, and methanesulfonyl chloride using the procedure described in Step 2 of Preparation A1. Recrystallization from EtOH provided the title compound. 1HNMR (400 MHz, CDCl3) δ6.93 (m, 1H), 6.74 (m, 2H), 5.09 (m, 1H), 4.01 (t, 2H), 3.47 (q, 2H), 2.96 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344485B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-24b8ac2f76f44da986b78595515a6f77 |
| Source note | uspto-grants-2002_02 |