HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 86757765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Product | HCID 86757765 | HCID 86757765 | — |
Reaction Steps
44.5 g (150 mmol) of triphosgene (98% pure according to HPLC) were dissolved in 120 ml of absolute tetrahydrofuran (THF) in a 250 ml dropping funnel having a pressure balance. In so doing, no heating or gas evolution was observed. About 150 ml of triphosgene/THF solution were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344565B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-f58428745c3542198865da14a6aa8938 |
| Source note | uspto-grants-2002_02 |