Ethyl Bromide → HCID 178420660, compound

Participants

Reaction Steps

Initially, a 13% by weight ethylmagnesium bromide-tetrahydrofuran solution was prepared from ethyl bromide and metallic magnesium, and 61.51 g (0.060 mol) of the solution was placed in a flask. To this solution was added dropwise a solution of 4.76 g (0.02 mol) of n-butyl 1-adamantanecarboxylate in 7.21 g of tetrahydrofuran while maintaining the inner temperature not exceeding 35° C., followed by stirring at room temperature for 1 hour.

Provenance & Evidence