HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18321485, compound → tert-Butyl 4-(piperidin-4-yl)piperazine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18321485 | HCID 18321485 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | tert-Butyl 4-(piperidin-4-yl)piperazine-1-carboxylate | HCID 17750356 | 79.7% |
Reaction Steps
Prepared analogously to Example A3f) from 1-(1,1-dimethylethoxycarbonyl)-4-[1-(phenylmethyl)-4-piperidinyl]piperazine by hydrogenolysis, but using Pearlman's catalyst instead of palladium/charcoal, in a yield of 79.7% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06344449B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-e521d7ae37144e2fa700680197cbf078 |
| Source note | uspto-grants-2002_02 |