HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18319637, compound → HCID 18319549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18319637 | HCID 18319637 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Product | HCID 18319549 | HCID 18319549 | 96.3% |
Reaction Steps
A mixture of ethyl 2,3-dihydro-9-hydroxymethyl-1-benzoxepin-4-carboxylate (0.45 g) and manganese (IV) oxide (4.5 g) was stirred under reflux for 1 hour and filtered off. The filtrate was evaporated in vacuo to give a solid of ethyl 2,3-dihydro-9-formyl-1-benzoxepin-4-carboxylate (0.43 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06346527B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-6af95d4826784047ac077d193790cff0 |
| Source note | uspto-grants-2002_02 |