HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 9859145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 54348027 | HCID 54348027 | — |
| Product | HCID 9859145 | HCID 9859145 | 35% |
Reaction Steps
5-Chloro-1-(dimethylamino)-4H-quinoline was prepared in the same manner as in Example 1 except that 3-(2,6-dichlorophenyl)propionaldehyde N,N-dimethylhydrazone was used in place of 2-chlorophenylacetaldehyde N,N-dimethylhydrazone, cesium carbonate was used in place of t-butoxysodium, and the reaction was conducted at 120° C. for 8 hours. (Yield: 35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06346621B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-4fc34f26134b47269ba476ee7c186808 |
| Source note | uspto-grants-2002_02 |