HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxytetrahydrofuran → HCID 15860435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxytetrahydrofuran | HCID 79098 | — |
| Reactant | HCID 18320646 | HCID 18320646 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 15860435 | HCID 15860435 | 86% |
Reaction Steps
The pyrrole ring was assembled by reacting 3,3-dimethyl-2-[3-(4-(1-naphthyl)-1-piperazinyl)prop-1-yl]-6-amino-2,3-dihydro-1,2-benzoisothiazole 1,1-dioxide with 2,5-dimethoxytetrahydrofuran in glacial acetic acid at 100° C. (1 h) in 86% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06346622B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-30d6dad6ab7841168e53446254690aff |
| Source note | uspto-grants-2002_02 |