HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl pyruvate → HCID 22388504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl pyruvate | HCID 11748 | — |
| Reactant | HCID 22387919 | HCID 22387919 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22388504 | HCID 22388504 | — |
Reaction Steps
A mixture of ethyl 4-amino-3-(2,4-dichlorobenzylamino)benzoate (1.90 g) and methyl pyruvate (0.55 ml) in toluene (15 ml) was heated under reflux for 1 hr. The reaction mixture was concentrated. The residue was washed with methanol and dried to give the object compound (0.50 g) as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06348474B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-708b1739226743b98f0b292a186e2516 |
| Source note | uspto-grants-2002_02 |