HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11109189, compound → HCID 11065720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11109189 | HCID 11109189 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 11065720 | HCID 11065720 | 7.5% |
Reaction Steps
A solution of 5-(2-chlorophenyl)-3-(2-oxopropylthio)-2-cyclohexen-1-one (1.0 g) in xylene (10 ml) was refluxed for 7.5 days and cooled, and the reaction solution was purified with silica gel column chromatography (EtOAc/hexane) to give oil of 6-(2-chlorophenyl)-3-methyl-4,5,6,7-tetrahydrobenzothiophene-4-one (0.07 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350749B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-4e522adf603a4af88e33087f0c6a68c1 |
| Source note | uspto-grants-2002_02 |