HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 18318530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 18318442 | HCID 18318442 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18318530 | HCID 18318530 | 100% |
Reaction Steps
A mixture of 3-[4-(2-ethoxy-2-oxoethoxy)benzyl]-2-[4-[2-(1-pyrrolidinyl)ethoxy]phenyl]benzo[b]thiophene (400 mg), hydrazine hydrate (2 mL), and EtOH (50 mL was refluxed for 3.5 hours, cooled, and evaporated in vacuo to give the title compound as an amorphous solid (0.4 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350774B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-1628ad441dd342eca122ca4d7759728d |
| Source note | uspto-grants-2002_02 |