HCID 15453526, compound → HCID 15453527, compound

Participants

Reaction Steps

0.15 g of 10% palladium-on-charcoal is added to a solution of 0.53 g of 2-[2-(isopropoxy-5-vinylphenoxy)ethyl]isoindole-1,3-dione (1.51 mmol) in 8 ml of methanol. The suspension is stirred under a hydrogen atmosphere for 2 hours, the solid is then removed by filtration on a silica filter, and the solvent is evaporated off. The title product is isolated by crystallization from a cyclohexane/ethyl acetate mixture. 0.53 g of a white solid is obtained:

Provenance & Evidence