HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodododecane → 3-[Dodecyl(methyl)amino]propan-1-OL
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodododecane | HCID 20282 | — |
| Reactant | 3-(Methylamino)-1-propanol | HCID 10148986 | — |
| Product | 3-[Dodecyl(methyl)amino]propan-1-OL | HCID 13122261 | 96% |
Reaction Steps
A solution of 3-(methylamino)propanol (5.71 g, 64.0 mmol, S. Koepke, R. Kupper, and C. J. Michejda, J. Org. Chem., 44, 2718,1979)), and iodododecane (7.58 g, 25.6 mmol) was reacted as described in example 1 to give 6.33 g (96%) of the title material as an oil, b.p. 100-105° C./0.04 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350892B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-21879c34c41243e6a2c2f4986c2992ea |
| Source note | uspto-grants-2002_02 |