HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 131723125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (2-Bromoethoxy)(tert-butyl)diphenylsilane | HCID 10915442 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131723125 | HCID 131723125 | — |
Reaction Steps
A mixture of methyl 4-hydroxybenzoate (3.25 g, 22.0 mmol, 2-(tert-butyldiphenylsilyloxy) ethyl bromide (8.0 g, 22.0 mmol, powdered anhydrous potassium carbonate (12 g) and potassium iodide (0.1 g) in acetone (250 ml) was heated under reflux for 48 h. The solid was then filtered and the filtrate was evaporated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06350892B1 |
| Source dataset | uspto-grants-2002_02 |
| ORD ID | ord-fbe4bd08cf394f059711518b7bd8b379 |
| Source note | uspto-grants-2002_02 |