1-Naphthalenamine, 4-(phenylazo)- → HCID 54163507, compound

HRID 1701153Notes

Reaction equation

HRID 1701153 reaction equation
[C:1]1([N:7]=[N:8][C:9]2[C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[C:12]([NH2:19])=[CH:11][CH:10]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:20]([O:27][C:28]([N:30]1[CH2:37][CH2:36][CH2:35][C@H:31]1[C:32](O)=[O:33])=[O:29])[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:1]1([N:7]=[N:8][C:9]2[C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[C:12]([NH:19][C:32](=[O:33])[C@@H:31]3[CH2:35][CH2:36][CH2:37][N:30]3[C:28]([O:27][CH2:20][C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[O:29])=[CH:11][CH:10]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 85621-Naphthalenamine, 4-(phenylazo)-HCID 101987Benzyloxycarbonyl-L-proline

Product 1

HCID 54163507HCID 54163507, compound

Procedure

4-Phenylazo-1-naphthylamine (4.9 g, 0.02 mole) and N-benzyloxylcarbonyl-L-proline (5.0 g, 0.02 mole) were coupled and the reaction mixture was worked up as in Example 6. The final product was obtained as crystals.

Sources & evidence

ORD record
ord-8f7ae20cba234216add3d00373506eb7
Source dataset
uspto-grants-1980_03
Patent number
US04191808

Reaction notes

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