HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 21527339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 53960187 | HCID 53960187 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21527339 | HCID 21527339 | — |
Reaction Steps
A mixture of 2.0 g. of [2-carbamyl-3-(methylthio)phenyl] oxamic acid ethyl ester and 1.44 g. of m-chloroperoxybenzoic acid in 200 ml. of methylene chloride is stirred for 2 hours. 0.6 g. of sodium bicarbonate in 20 ml. of water is added, the methylene chloride layer is separated, dried and evaporated. The residue is recrystallized from ethanol-diethyl ether, m.p. 164°-166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04191840 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-b9999489eaca44b69762bc70d2dfe458 |
| Source note | uspto-grants-1980_03 |