Water → HCID 88776755, compound

HRID 1701263Notes

Reaction equation

HRID 1701263 reaction equation
[C:1]([CH2:4][CH2:5][P:6]([CH2:21][C:22]1[CH:27]=[C:26]([C:28]([CH3:31])([CH3:30])[CH3:29])[C:25]([OH:32])=[C:24]([C:33]([CH3:36])([CH3:35])[CH3:34])[CH:23]=1)([CH2:8][CH2:9][C:10]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[O:11])=[O:7])(=[O:3])N.[OH2:37]>CCCCC>[C:33]([C:24]1[CH:23]=[C:22]([CH:27]=[C:26]([C:28]([CH3:31])([CH3:30])[CH3:29])[C:25]=1[OH:32])[CH2:21][P:6]([CH2:8][CH2:9][C:10]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[O:11])([CH2:5][CH2:4][C:1]([O:37][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[O:3])=[O:7])([CH3:36])([CH3:35])[CH3:34]

Participants

4

Reactant 2

HCID 962WaterHCID 131711726HCID 131711726, compound

Product 1

HCID 88776755HCID 88776755, compound

Reagents, catalysts & solvents 1

HCID 8003PentaneSolvent

Procedure

The filtrate from Example 2, containing water and pentane, is recovered and the water layer is separated. The pentane layer is then heated to strip off pentane and obtain 5.1 grams of a yellow oil which is further heated at 180° C. under a 1 mm. vacuum to remove volatile materials and obtain the desired product.

Workup

  1. customis recovered
  2. customthe water layer is separated
  3. temperatureThe pentane layer is then heated

Sources & evidence

ORD record
ord-84122670a83e4685983953c46e68a931
Source dataset
uspto-grants-1980_03
Patent number
US04192796

Reaction notes

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