Allylamine → HCID 178457547, compound

HRID 1701322Notes

Reaction equation

HRID 1701322 reaction equation
[CH2:1]([NH2:4])[CH:2]=[CH2:3].[C:5]([NH:7][C:8](=[N:11][CH2:12][CH2:13][S:14][CH2:15][C:16]1[NH:20][CH:19]=[N:18][C:17]=1[CH3:21])SC)#[N:6]>C(#N)C>[CH2:1]([NH:4][C:8]([NH:7][C:5]#[N:6])=[N:11][CH2:12][CH2:13][S:14][CH2:15][C:16]1[NH:20][CH:19]=[N:18][C:17]=1[CH3:21])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 7853AllylamineHCID 178503877HCID 178503877, compound

Product 1

HCID 178457547HCID 178457547, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Reaction of allylamine and N-cyano-N'-[2-((4-methyl-5-imidazolyl)methylthio)ethyl]-S-methylisothiourea by the procedure of Example 11 afforded the title compound, m.p. 113°-114° C. (from acetonitrile).

Sources & evidence

ORD record
ord-162554da65de4884b696de5e55ff209f
Source dataset
uspto-grants-1980_03
Patent number
US04192879

Reaction notes

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