HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-Nitro-indan-2-ylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-(5-nitro-indan-2-yl)-acetamide | HCID 14820512 | — |
| Product | 5-Nitro-indan-2-ylamine hydrochloride | HCID 22319324 | — |
Reaction Steps
N-Acetyl-5-nitro-2-indanamine, 1.5 g. (0.007 mole) as prepared in Example 9 was refluxed in 10% hydrochloric acid for 3 hours. The mixture was evaporated and the crystalline residue recrystallized from methanol-ether to yield 5-nitro-2-indanamine hydrochloride, dec.>280° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04192888 |
| Source dataset | uspto-grants-1980_03 |
| ORD ID | ord-00640c1748ab49b6be035facddf7563e |
| Source note | uspto-grants-1980_03 |