HRID1701345

反应详情

EQUATION

反应方程式

HRID 1701345 的结构方程式

PROCEDURE

实验过程

N-Acetyl-5-nitro-2-indanamine, 1.5 g. (0.007 mole) as prepared in Example 9 was refluxed in 10% hydrochloric acid for 3 hours. The mixture was evaporated and the crystalline residue recrystallized from methanol-ether to yield 5-nitro-2-indanamine hydrochloride, dec.>280° C.

WORKUP

后处理

  1. custom(0.007 mole) as prepared in Example 9
  2. customThe mixture was evaporated
  3. customthe crystalline residue recrystallized from methanol-ether