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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1701480Generated: October 31, 2026

1-(3-Chlorophenyl)-3-hydroxyurea → HCID 13071780, compound

https://huagongshe.com/reaction/1701480

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(3-Chlorophenyl)-3-hydroxyureaHCID 269503—
SolventEthyl ketoneHCID 7288—
ProductHCID 13071780HCID 13071780—

Reaction Conditions

Temperature90 °C

Reaction Steps

18.7 g. of N-(3-chlorophenyl)-N'-hydroxy-urea are added to 116 g. of diethyl ketone. The reaction is stirred at 90° C. for 1 hour. The reaction mixture is then evaporated to dryness and the residue is recrystallized from a mixture of methanol and water.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04193922
Source datasetuspto-grants-1980_03
ORD IDord-82f7474bc18e4c51b89226b8f96ff34c
Source noteuspto-grants-1980_03